edited by Roderick E. Wasylishen, Sharon E. Ashbrook, Stephen Wimperis
Hardcover: 550 pages
Publisher: Wiley; August 2012
Language: English
ISBN: 978-0470973981 http://www.amazon.com/dp/0470973986 http://www.amazon.ca/dp/0470973986
Wiley: Many important materials do not contain spin-1/2 nuclei traditionally investigated by NMR spectroscopy and secondly, dissolving solid materials in a solvent may be impossible or may destroy the integrity of the material. All these obstacles can be overcome by NMR experiments at high-magnetic field strengths and investigating the properties of quadrupolar nuclei.
This Handbook gives an up-to-date account of NMR of quadrupoloar nuclei in the solid state. Each chapter of the Handbook has been prepared by an expert who has made significant contributions to our understanding and appreciation of the importance of NMR studies of quadrupolar nuclei in solids.
The text is divided into three Parts:
A) Basic Principles of Quadrupolar NMR
B) Advanced Solid-State NMR Techniques to Investigate Quadrupolar Nuclei
C) Applications Involving NMR Studies of Quadrupolar Nuclei in Solids.
The first section provides the reader with the background necessary to appreciate the challenges in acquiring and interpreting NMR spectra of quadrupolar nuclei in solids. The second section presents cutting-edge techniques and methodology for employing these spectroscopic techniques to investigate quadrupolar nuclei in solids. The final section explores applications of solid-state NMR studies of solids ranging from investigations of biological samples to porous materials, catalysts, geological samples and high-temperature superconductors.
[NMR900 blog] Solid-State NMR in Materials for Energy Storage and Conversion
Solid-State NMR in Materials for Energy Storage and Conversion
A special issue of Solid State Nuclear Magnetic Resonance guest-edited by Clare Grey (Cambridge) and Gillian Goward (McMaster), Volume 42, Pages 1-98 (April 2012) http://www.sciencedirect.com/science/journal/09262040/42
Editorial
Clare P. Grey, Gillian R. Goward, Editorial "Solid-State NMR in Materials for Energy Storage and Conversion," Solid State Nuclear Magnetic Resonance
42 (2012) 1. http://dx.doi.org/10.1016/j.ssnmr.2012.03.001
Canadian contributions
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News from NMR blogs
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03-21-2012 11:40 PM
Rapid Solid-State NMR of Deuterated Proteins by Interleaved Cross-Polarization fromH andH Nuclei
Rapid Solid-State NMR of Deuterated Proteins by Interleaved Cross-Polarization fromH andH Nuclei
Publication year: 2011
Source: Journal of Magnetic Resonance, Available online 9 November 2011</br>
Morten*Bjerring, Berit*Paaske, Hartmut*Oschkinat, Umit*Akbey, Niels Chr.*Nielsen</br>
We present a novel sampling strategy, interleaving acquisition of multiple NMR spectra by exploiting initial polarization subsequently fromH andH spins, taking advantage of their differentT1relaxation times. DifferentH- andH-polarization based spectra are in this way simultaneously recorded improving either...
[NMR paper] Low temperature solid-state NMR experiments of half-integer quadrupolar nuclides: cav
Low temperature solid-state NMR experiments of half-integer quadrupolar nuclides: caveats and data analysis.
Related Articles Low temperature solid-state NMR experiments of half-integer quadrupolar nuclides: caveats and data analysis.
J Magn Reson. 2004 May;168(1):66-74
Authors: Lipton AS, Heck RW, Sears JA, Ellis PD
Solid-state NMR spectroscopy of half-integer quadrupolar nuclides has received a lot of interest recently with the advent of new methodologies and higher magnetic fields. We present here the extension of our previous low...
nmrlearner
Journal club
0
11-24-2010 09:51 PM
New NMR Book: Solid-State NMR Studies of Biopolymers
New NMR Book: Solid-State NMR Studies of Biopolymers
edited by Anne McDermott, Tatyana Polenova
Hardcover: 592 pages
Publisher: Wiley; September 2010
Language: English
ISBN: 978-0470721223
http://www.amazon.com/dp/0470721227
http://www.amazon.ca/dp/0470721227
nmrlearner
Books
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10-05-2010 02:04 AM
[U. of Ottawa NMR Facility Blog] Solid State NMR of Half Integer Quadrupolar Nuclei
Solid State NMR of Half Integer Quadrupolar Nuclei
Many students who do liquid state NMR or solid state NMR of spin I=1/2 nuclei have very little appreciation for the information content and complexity of the solid state NMR spectra of spin I = n/2 quadrupolar nuclei (n= 3, 5, 7....). In part, I think this may be due to the mathematics involved with explaining the important effects. With this post, I attempt to describe the NMR spectrum of an I = 5/2 nucleus in the soild state without resorting to mathematics. I hope that this post helps to boost the understanding and appreciation for the...
New book: NMR of Quadrupolar Nuclei in Solid Materials
Linear Mode
