Pulse sequence for homonuclear correlation with SPC5 mixing period
Pulse sequence for homonuclear correlation with SPC5 mixing period
Hi,I'm looking for a pulse program suitable for Bruker Avance llI (topspin 2.1) which is 2D homonuclear correlation with a mixing period of the symmetry based pulse scheme - the SPC5 scheme. I took the basic PDSD experiment and just replaced the mixing period with the appropriate pulses of the SPC5 scheme but it didn't work. Does someone has a ready-to-run pulse scheme out there? Basically for 13C-13C correlation, the program starts with a 90 pulse on 1H, followed by CP from 1H to 13C, t1 evolution, 90 pulse on 13C, mixing SPC5, and another 90 pulse and detection. Check if somebody has answered this question on NMRWiki QA forum |
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