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[Question from NMRWiki Q&A forum] Pulse sequence for homonuclear correlation with SPC5 mixing period

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09-27-2012, 03:49 PM

nmrlearner

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Pulse sequence for homonuclear correlation with SPC5 mixing period

Pulse sequence for homonuclear correlation with SPC5 mixing period

Hi,I'm looking for a pulse program suitable for Bruker Avance llI (topspin 2.1) which is 2D homonuclear correlation with a mixing period of the symmetry based pulse scheme - the SPC5 scheme. I took the basic PDSD experiment and just replaced the mixing period with the appropriate pulses of the SPC5 scheme but it didn't work. Does someone has a ready-to-run pulse scheme out there? Basically for 13C-13C correlation, the program starts with a 90 pulse on 1H, followed by CP from 1H to 13C, t1 evolution, 90 pulse on 13C, mixing SPC5, and another 90 pulse and detection.

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