Thread: NMR paper Transverse dephasing optimized solid-state NMR spectroscopy.
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Default Transverse dephasing optimized solid-state NMR spectroscopy.
Transverse dephasing optimized solid-state NMR spectroscopy.

Related Articles Transverse dephasing optimized solid-state NMR spectroscopy.

J Am Chem Soc. 2003 Nov 19;125(46):13938-9

Authors: De Paëpe G, Giraud N, Lesage A, Hodgkinson P, Böckmann A, Emsley L

It is shown how coherence lifetimes in solid-state NMR experiments can be controlled. New decoupling schemes are introduced which actively optimize dephasing times, providing increases of up to a factor of 2 with respect to the best existing schemes. The new schemes are implemented in transverse-dephasing-optimized (TDOP) NMR experiments for the disorded solid cellulose, and for a microcrystalline protein, where sensitivity improvements of up to a factor of 5 are obtained.

PMID: 14611212 [PubMed - indexed for MEDLINE]



Source: PubMed
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