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kcsham2 05-22-2013 07:42 AM

How to obtain a good COSY spectrum of a paramagnetic compound
 
How to set up the experiment in order to obtain a good COSY spectrum of compound that containing Cu(II), which should hyperfine shift from 150ppm to -50 ppm?

I have tried to do it by just changing the spectrum width of both dimension, with an hour of acquistion time, but no cross peak can be observed between any signal.


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