Why do we trun off sample spinning when we do NOESY experiment?
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Magic Angle Spinning and Oriented Sample Solid-State NMR Structural Restraints Combine for Influenza A M2 Protein Functional Insights
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nmrlearner
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05-25-2012 07:14 PM
[Question from NMRWiki Q&A forum] Why do we trun off sample spinning when we do NOESY experiment?
Why do we trun off sample spinning when we do NOESY experiment?
Why do we trun off sample spinning when we do NOESY experiment?
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nmrlearner
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05-25-2012 07:14 PM
[Question from NMRWiki Q&A forum] spinning heating sample in MAS
spinning heating sample in MAS
there are two known mechanisms: friction heating( which may cause several degrees temperature increase) and induced AC current heating( in this paper:Electrical and ionic conductivity effects on magic-angle spinning nuclear magnetic resonance parameters of CuI. which can heat sample over 100 Celsius.)My question is, has any body seen this heating in MAS NMR?
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nmrlearner
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04-30-2012 05:23 AM
[NMRpipe Yahoo group] Re: A sample 4D HCCH Noesy spectrum
Re: A sample 4D HCCH Noesy spectrum
This is an example for an HN-Methyl 4D I have, not exactly the same, but perhaps useful to see anyway ... the processing scheme is a very basic one ...
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12-13-2011 02:46 AM
[NMRpipe Yahoo group] Re: A sample 4D HCCH Noesy spectrum
Re: A sample 4D HCCH Noesy spectrum
Hi Have you tried the example from NMRDraw macro editor? (under process 4D) I believe nothing is special in term of processing data. Phasing, sweep width, and
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12-10-2011 02:38 AM
[NMRpipe Yahoo group] A sample 4D HCCH Noesy spectrum
A sample 4D HCCH Noesy spectrum
Hello, I'm struggling to process a 4D methyl noesy spectrum collected on a Bruker and I was wondering if anyone knows where I could find an example ser file
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12-10-2011 02:38 AM
[NMR paper] The 3D NOESY-[(1)H,(15)N,(1)H]-ZQ-TROSY NMR experiment with diagonal peak suppression
The 3D NOESY--ZQ-TROSY NMR experiment with diagonal peak suppression.
Related Articles The 3D NOESY--ZQ-TROSY NMR experiment with diagonal peak suppression.
Proc Natl Acad Sci U S A. 1999 Aug 17;96(17):9607-12
Authors: Pervushin KV, Wider G, Riek R, Wüthrich K
In our 3D NOESY--ZQ-TROSY experiment, the TROSY principle (transverse relaxation-optimized spectroscopy) is used in three-dimensional (3D) (15)N-resolved nuclear Overhauser enhancement spectroscopy (NOESY), which enables resonance assignments by sequential nuclear Overhauser effects and...
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11-18-2010 08:31 PM
[NMR paper] Proton NMR studies of a large protein. pH, substrate titrations, and NOESY experiment
Proton NMR studies of a large protein. pH, substrate titrations, and NOESY experiments with perdeuterated yeast phosphoglycerate kinase containing histidine residues.
Related Articles Proton NMR studies of a large protein. pH, substrate titrations, and NOESY experiments with perdeuterated yeast phosphoglycerate kinase containing histidine residues.
J Magn Reson B. 1994 Oct;105(2):157-66
Authors: Pappu KM, Serpersu EH
Fully deuterated yeast phosphoglycerate kinase (PGK) was prepared biosynthetically with only histidine side chains of normal...