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nmrlearner

08-21-2011 04:55 AM

Help for Boron 11 NMR!

Help for Boron 11 NMR!

I'm using a Bruker 300 NMR, equipped with a BBO probe, to do Boron 11 NMR. But I got no signal no matter what pulse length or scan width I set, I don't know whether it's related with the borosilicate tubes I use, or should I use quartz ones. Could someone here give me some advice? Thank you!

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