BioNMR - Question from NMRWiki Q&A forum 31p-31p cosy

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nmrlearner

03-31-2015 06:18 AM

31p-31p cosy

31P-31P COSY

I like to run a 31P-31P COSY experiment to determine whether there is coupling between 1R-31P-CH2-31P-X in my molecule. I already have 1H decoupled 31P-spectra, showing two very different chemical shifts for these two 31P. However, I never run 31P-31P COSY before, anyone have any advises. I have Bruker Avance II instrument. Thanks.

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