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-   -   [NMR paper] Quantitative analysis of Bordeaux red wine precipitates by solid-state NMR: Role of tartrates and polyphenols. (http://www.bionmr.com/forum/journal-club-9/quantitative-analysis-bordeaux-red-wine-precipitates-solid-state-nmr-role-tartrates-polyphenols-23091/)

nmrlearner 01-19-2016 07:37 PM

Quantitative analysis of Bordeaux red wine precipitates by solid-state NMR: Role of tartrates and polyphenols.
 
Quantitative analysis of Bordeaux red wine precipitates by solid-state NMR: Role of tartrates and polyphenols.

Related Articles Quantitative analysis of Bordeaux red wine precipitates by solid-state NMR: Role of tartrates and polyphenols.

Food Chem. 2016 May 15;199:229-37

Authors: Prakash S, Iturmendi N, Grelard A, Moine V, Dufourc E

Abstract
Stability of wines is of great importance in oenology matters. Quantitative estimation of dark red precipitates formed in Merlot and Cabernet Sauvignon wine from Bordeaux region for vintages 2012 and 2013 was performed during the oak barrel ageing process. Precipitates were obtained by placing wine at -4°C or 4°C for 2-6days and monitored by periodic sampling during a one-year period. Spectroscopic identification of the main families of components present in the precipitate powder was performed with (13)C solid-state CPMAS NMR and 1D and 2D solution NMR of partially water re-solubilized precipitates. The study revealed that the amount of precipitate obtained is dependent on vintage, temperature and grape variety. Major components identified include potassium bitartrate, polyphenols, polysaccharides, organic acids and free amino acids. No evidence was found for the presence of proteins. The influence of main compounds found in the precipitates is discussed in relation to wine stability.


PMID: 26775965 [PubMed - in process]



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