NMR paper Efficient heteronuclear decoupling in MAS solid-state NMR using non-rotor-synchronized rCW irradiation.

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[NMR paper] Efficient heteronuclear decoupling in MAS solid-state NMR using non-rotor-synchronized rCW irradiation.

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NMR processing:

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Side-chains:

NOEs:

Structure from NMR restraints:

Ab initio:

Fragment-based:

Rosetta-NMR (Robetta)

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Fragment-based:

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Promega- Proline

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TALOS

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d2D

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08-16-2014, 10:26 PM

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Efficient heteronuclear decoupling in MAS solid-state NMR using non-rotor-synchronized rCW irradiation.

Efficient heteronuclear decoupling in MAS solid-state NMR using non-rotor-synchronized rCW irradiation.

Related Articles Efficient heteronuclear decoupling in MAS solid-state NMR using non-rotor-synchronized rCW irradiation.

J Magn Reson. 2014 Jul 19;246C:104-109

Authors: Equbal A, Paul S, Mithu VS, Madhu PK, Nielsen NC

Abstract
We present new non-rotor-synchronized variants of the recently introduced refocused continuous wave (rCW) heteronuclear decoupling method significantly improving the performance relative to the original rotor-synchronized variants. Under non-rotor-synchronized conditions the rCW decoupling sequences provide more efficient decoupling, are easier to setup, and prove more robust towards experimental parameters such as radio frequency (rf) field amplitude and spinning frequency. This is demonstrated through numerical simulations substantiated with experimental results under different sample spinning and rf field amplitude conditions for powder samples of U-(13)C-glycine and U-(13)C-L-histidine·HCl·H2O.

PMID: 25123538 [PubMed - as supplied by publisher]

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