1H-detected characterization of carbon-carbon networks in highly flexible protonated biomolecules using MAS NMR
1H-detected characterization of carbon-carbon networks in highly flexible protonated biomolecules using MAS NMR
In the last three decades, the scope of solid-state NMR has expanded to exploring complex biomolecules, from large protein assemblies to intact cells at atomic-level resolution. This diversity in macromolecules frequently features highly flexible components whose insoluble environment precludes the use of solution NMR to study their structure and interactions. While High-resolution Magic-Angle Spinning (HR-MAS) probes offer the capacity for gradient-based ¹H-detected spectroscopy in solids, such... More... |
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